205877-26-5 4-乙炔基三苯胺

危险性质：非危险化学品

未明确提及具体用途

未明确提及具体应用领域

合成路线 1（1. 合成：205877-26-5）

产率：93% 合成条件：With tetrabutyl ammonium fluoride In tetrahydrofuran at 20℃; for 5 h; 实验步骤：将1.0g（2.93mmol）中间体6（1）溶解在10.0mL THF中，在室温下向其中逐渐加入14.64mL（14.64mmol）1.0M四丁基氟化铵的THF溶液，然后搅拌混合物 在室温下保持5小时。 反应结束后，加入50mL蒸馏水，用50mL二氯甲烷萃取3次，得到有机层。 收集有机层并用硫酸镁干燥以蒸发溶剂。 使用硅胶柱色谱法分离纯化残余物，得到730mg（2.78mmol）中间体6（2）（产率：93％）。 使用LC-MS鉴定产生的化合物。 C20H15N：M + 270.12 参考文献：

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