- 急性毒性
口服-大鼠 LD:>500 毫克/公斤;静脉-小鼠 LD50: 100 毫克/公斤
- 可燃性危险特性
热分解排出有毒溴化物和氮氧化物烟雾
- 储运特性
库房通风低温干燥
- 灭火剂
水,干粉、干砂、二氧化碳、泡沫、1211灭火剂
医药; 农药
合成路线 1（1. 合成：13296-94-1）
产率：99%
合成条件：With pyrrolidone hydrotribromide In methanol; dichloromethane at 20℃; for 0.50 h;
实验步骤：在室温下，用PHT（6.30g，12.7mmol，1.1当量）处理4-硝基苯胺（1.60g，11.6mmol，1当量）在DCM（40mL）和MeOH（20mL）中的溶液。 方式。 然后继续搅拌0.5小时。 将混合物用Et 2 O（50mL）稀释，先用饱和Na 2 S 2 O 3水溶液（40mL）洗涤，然后用盐水（40mL）洗涤。 将有机萃取物用MgSO 4干燥，然后过滤并减压除去溶剂。 通过快速柱色谱法（c-Hex-EtOAc; 2：1）纯化，得到S8（2.50g，99％），为黄色固体。
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