78600-31-4 2-溴三苯胺

常温运输，非危险化学品，海关编码2921.49.5000

主要用于化学合成与材料科学领域。

化学合成; 材料科学

路线1：

• 步骤: 将30g（0.177mol）二苯胺、49g（0.355mol）碳酸钾和3.5g（0.035mol）氯化铜加入500mL圆底烧瓶中，加入300mL二甲基亚砜，再加入75.2g（0.266mol）2-溴碘苯，混合物回流12小时。反应完成后冷却至室温，萃取，减压浓缩有机层，用己烷重结晶，干燥得48.1g（83.7%）目标化合物。
• 条件: 以碳酸钾、氯化铜为催化剂，二甲基亚砜为溶剂，回流12小时。
• 产率: 83.7%
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