60974-92-7 9,10-双(二乙基膦甲基)蒽

常温运输，危险性质为非危险化学品，海关编码2931.90.6000。

化学合成

化学合成

合成路线 1（1. 合成：60974-92-7）

• 步骤: 将9,10-双（氯甲基）蒽（7.8g，28.3mmol）和亚磷酸三乙酯（30mL）的溶液在温和回流下剧烈搅拌过夜；通过减压蒸馏除去过量的亚磷酸三乙酯；通过硅胶柱色谱法分离粗产物，使用乙酸乙酯/石油醚（1/1，v/v）作为洗脱剂。
• 条件: Reflux
• 收率: 76.8%
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合成路线 2（2. 合成：60974-92-7）