化学合成。
化学合成
合成路线 1（1. 合成：26032-72-4）
产率：82%
合成条件：With tetrakis(triphenylphosphine) palladium (0) ; potassium carbonate In tetrahydrofuran; water for 5 h; Inert atmosphere; Heating
实验步骤：在氮气氛下，将2,4,6-三氯嘧啶（40.0g，0.218mol）和苯基硼酸（26.6g，0.218mol）完全溶解在250mL四氢呋喃中，加入2M碳酸钾水溶液（125mL）和四（三苯基膦）。 然后加热钯（7.6g，6.5mmol）并搅拌5小时。 将温度降至室温，除去水层，用无水硫酸镁干燥，减压浓缩，并用1：3比例的四氢呋喃和己烷的柱处理，制得化合物6-A（40g，产率） ：82％）。
参考文献：
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