化学合成；生命科学。
化学合成; 生命科学
合成路线 1（1. 合成：14316-06-4）
产率：99%
合成条件：at 20℃; for 2 h;
实验步骤：通用程序：将SOCl 2（21.8mL，0.3mol）和（S） - 丙氨酸（（S）-19,8.91g，0.1mol）加入到CH 3 OH（100mL）中并将混合物在室温下搅拌2小时。 真空除去溶剂，将残余物溶于甲醇（30mL）中，再次真空除去有机溶剂。 该过程重复两次。 无色无定形固体，熔点103℃（参考39℃98-99℃），产量14.3g（> 99％）。
参考文献：
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