化学合成。
化学合成
合成路线 1(1. 合成:14543-43-2)
产率:100%
合成条件:With hydrogen In methanol; Pd on active carbon
实验步骤:3-氨基-4-羟基苄腈的制备。 在室温下,在5%Pd /活性炭(0.5g)存在下,用氢气通过气球处理4-羟基-3-硝基苄腈(10g,61mmol)的MeOH(200mL)溶液24小时。 过滤混合物,浓缩滤液,得到产物(8.2g,100%)。
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