化学合成。
化学合成
合成路线 1（1. 合成：61032-42-6）
产率：99.4%
合成条件：With iron; ammonium chloride In methanol; water at 80℃; for 0.50 h; Inert atmosphere
实验步骤：8.0g化合物II，12.0g铁粉，12.0g氯化铵，60ml水，120ml二氯甲烷。将醇的混合物在80℃下回流搅拌30分钟。 TLC分析显示没有起始原料，用50ml甲醇和50ml乙酸乙酯滤出，将滤液旋转干燥，将溶剂加入300ml水，乙酸乙酯中，并用饱和洗涤有机相。 氯化钠溶液，用无水硫酸镁干燥，干燥，得到7.2g棕色固体（化合物3），产率99.4％;
参考文献：
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