化学合成。
化学合成
合成路线 1(1. 合成:108940-96-1)
产率:100%
合成条件:With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 15 h; Inert atmosphere
实验步骤:将2,4-二溴-3-甲氧基 - 苯甲醛(化合物1)溶于无水DMF中,加入过量的甲基碘和碳酸钾,在室温下在氮气下搅拌过夜,萃取得到化合物2。
参考文献:
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