化学合成。
化学合成
合成路线 1（1. 合成：29671-92-9）
产率：96.64%
合成条件：With hydrogenchloride In diethyl ether at 5 - 20℃;
实验步骤：例6; 盐酸氯甲脒的合成; 将氰胺（50.0g，1.19mol，1当量）在二乙醚（900ml）中的溶液冷却至0℃，然后加入氯化氢的乙醚溶液（450g，29％），保持温度低于+ 5℃。 加完后，将得到的白色悬浮液在室温下进一步搅拌一小段时间，滤出白色沉淀并在30℃下真空干燥。 获得白色固体（132.66g，1.15mol，96.64％）。
参考文献：
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