14062-25-0 对溴苯基乙酸乙酯

运输信息：常温运输。危险描述：危险性质为否，属于非危险品。

化学合成

化学合成

路线1：2-(4-溴苯基)乙酸与乙醇酯化法

• 步骤：将2-(4-溴苯基)乙酸（75g，340mmol）悬浮在乙醇（341mL）中，加入浓硫酸（0.682mL，12.79mmol），加热至回流24小时。浓缩反应物，残余物用乙醚和饱和碳酸氢钠稀释，分离有机层，盐水洗涤，硫酸钠干燥，过滤浓缩得产物（80.2g）。
• 条件：回流24小时
• 产率：97%
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