化学合成；生命科学。
化学合成；生命科学
合成路线 1（1. 合成：5619-09-0）
产率：100%
合成条件：Stage #1: With thionyl chloride In methanol; ethanol for 1 h; Cooling with ice Stage #2: at 20 - 66℃; for 6.50 h;
实验步骤：（2）L-色氨酸甲酯盐酸盐的制备在冰浴下，向100ml圆底烧瓶中加入60ml甲醇，然后通过恒压滴液漏斗（顶部带有干燥管）缓慢加入4ml SOCl2。 ）和NaOH溶液用于吸收废气。 搅拌1小时后，加入8mmol L-色氨酸（3d）并在室温下搅拌30分钟，然后在66℃下回流6小时。 通过TLC跟踪反应直至原料消失，用2％茚三酮在乙醇中的溶液作为显色剂。 蒸发溶剂，得到L-色氨酸甲酯盐酸盐。 产量：100％。
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