化学合成。
化学合成；钙钛矿电池研究
合成路线 1（1. 合成：775-00-8）
产率：97.89%
合成条件：With ammonia; hydrogen In methanol
实验步骤：将（4-三氟甲基 - 苯基） - 乙腈（2g，10.81mmol）的甲醇氨（50mL）溶液加入到在parr氢化器中的甲醇中的阮内镍（400mg）中。 将烧瓶在50PSI下搅拌过夜。 通过TLC（10％甲醇的CHCl 3溶液）监测反应。 将反应混合物通过硅藻土床过滤，将滤液减压干燥，得到2g产物（97.89％收率）.LCMS纯度：98.73％，m / z = 190.0（M + 1）
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