6941-75-9 5-溴异吲哚-1,3-二酮

中文名称: 5-溴异吲哚-1,3-二酮
英文名称: 4-Bromophthalimide
CAS号

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名称和标识

中文名: 5-溴异吲哚-1,3-二酮
英文名: 4-Bromophthalimide
CAS号: 6941-75-9
分子式: C8H4BrNO2
分子量: 226.03
中文别名: 4-溴邻苯二甲酰亚胺; 4-溴酞酰亚胺; 4-溴邻苯二甲酰亚; 4-邻苯二甲酰亚胺; 4-溴邻苯二亚胺
英文别名: 5-bromoisoindole-1,3-dione; 5-BROMO PHTHALIMIDE; bromophtalimide; 4-Bromophtalimide; 1H-Isoindole-1,3(2H)-dione, 5-broMo-; 4-Bromophthalimid; 5-bromopthalamide; 5-bromo-1,3-dihydro-1,3-dioxo-2H-isoindole; 5-Bromoisoindoline-1,3-dione; 1H-Isoindole-1,3(2H)-dione,5-broMo; 5-Bromo-1H-isoindole-1,3(2H)-dione; 5-Bromo-isoindole-1,3-dione

物化属性

LogP: 1.92
PSA: 46.17
外观: 米白色至淡黄色固体，无气味
密度: 1.8±0.1 g/cm3
折射率: 1.650
水溶解性

安全信息

安全说明

运输信息：常温运输。危险描述：非危险化学品，海关编码2933998090

生产及用途

用途与制备

化学合成；黄色至浅黄色粉末

化学合成

路线1：

步骤: 将中间体I-54（6.6g，0.30mol，1.0当量）和甲酰胺（10mL，2.4mol，8.0当量）的混合物在200℃下搅拌2小时并倒入冰水混合物中，过滤收集晶体并真空干燥，得到中间体I-55（7.0g，99％）。
条件: 200℃；2小时
收率: 99%
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