化学合成,医药中间体。
医药; 农药
合成路线 1(1. 合成:626-34-6)
产率:94%
合成条件:With ammonia In water
实验步骤:实施例9:制备氨基巴豆酸乙酯的方法连续流动实验在1.58mm o.d的SS316管式反应器中进行。 通过使用简单的T-混合器和1m长的反应器以1:3的比例混合乙酰乙酸乙酯与氨水(25%溶液),停留时间为22分钟。 产物产率在50℃时为94%。
参考文献:
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