化学合成。
农药; 化学合成
合成路线 1（1. 合成：5417-82-3）
产率：99%
合成条件：at 95℃; for 1.50 h; Neat (no solvent)
实验步骤：将丙二腈（17g，257.5λ7mmol）和原乙酸三乙酯（45.95g，283.25mmol）的混合物在95℃加热1.5小时。 然后将混合物真空蒸发，得到固体，将其滤出，得到化合物D1（34g，99％），为黄色固体。 该化合物无需进一步纯化即可用于下一反应步骤。化合物D1也可商购获得CAS：5417-82-3。
参考文献：
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