化学合成。
化学合成
合成路线 1（1. 合成：86521-05-3）
产率：95%
合成条件：at 20℃;
实验步骤：向2-溴吡啶（4.74g，0.030mol），CuI（0.14g，0-74mmol）和Pd（PPh 3）2 Cl 2（0.52g，0.74mmol）在100ml二异丙胺中的溶液中加入（三甲硅烷基甲硅烷基） ）乙炔（3.0g，0.030mol）。 将混合物在室温下在氮气氛下搅拌过夜。 在减压下除去溶剂后，通过减压蒸馏纯化残余物，得到5.0g（产率95％）纯化合物1的2-（三甲基甲硅烷基）吡啶。
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