181269-69-2 N-Boc-3-甲基-哌啶-4-酮

作为医药中间体，用于合成多种药物分子，具体应用可参考相关专利文献。

医药中间体

合成路线 1（1. 合成：181269-69-2）

产率：100% 合成条件：With hydrogen In ethyl acetate for 24 h; 实验步骤：将化合物28（15.0g，0.0738mol）和二碳酸二叔丁酯（17.7g，0.0812mol）溶解在EtOAc（400ml）中。 加入氢氧化钯催化剂（4g）并将混合物在Paar振荡器上在40psi氢气压下振荡24小时。 将所得混合物通过硅藻土过滤，并用EtOAc洗涤硅藻土。 浓缩滤液，得到15.73g（0.0738mol，100％）产物27B，为无色油状物。 MS（M-tBOC的ES + 1）：m / e 114 参考文献：

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