化学合成。
化学合成
合成路线 1（1. 合成：60032-63-5）
产率：72%
合成条件：With ammonium hydroxide; iodine; potassium iodide In water at 20℃; for 6 h;
实验步骤：向充分搅拌的KI（1.0mmol）和I 2（1.0mmol）的NH 4 OH（aq）溶液中加入30％（5.0ml）的对羟基苯甲醛（1.0mmol），使得到的混合物在室温下反应6小时。。 然后将溶液用HCl（水溶液）10％酸化，并用Et 2 O（2×10ml）萃取。 将合并的有机相用Na 2 SO 4干燥并蒸发至干。 从H 2 O中结晶后得到所需产物。 收率= 72％。 分析数据与已报道的相同化合物的数据相同.3分析。 C7H5IO2的计算值：C，33.90; H，2.03; O，12.90。 实测值：C，33.93; H，2.06，O，12.94。
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